6WMK
Crystal structure of beta sheet heterodimer LHD29
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-08-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.072, 38.175, 60.379 |
Unit cell angles | 90.00, 98.26, 90.00 |
Refinement procedure
Resolution | 38.030 - 2.200 |
R-factor | 0.2551 |
Rwork | 0.254 |
R-free | 0.28320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Designed Model |
RMSD bond length | 0.002 |
RMSD bond angle | 0.394 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18rc2_3793) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.220 | 2.310 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 12352 | 1996 |
<I/σ(I)> | 5.2 | 1 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 3.3 | 3 |
CC(1/2) | 0.971 | 0.468 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M Sodium Iodide, 20% PEG3350 |