6W2P
APE1 endonuclease product complex L104R
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-23 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 44.387, 61.780, 72.278 |
Unit cell angles | 83.71, 78.56, 88.02 |
Refinement procedure
Resolution | 24.450 - 1.940 |
R-factor | 0.2021 |
Rwork | 0.201 |
R-free | 0.23760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5dff |
RMSD bond length | 0.009 |
RMSD bond angle | 0.991 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX (1.17.1_3660) |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.980 |
High resolution limit [Å] | 1.940 | 1.950 |
Rmeas | 0.074 | 0.815 |
Number of reflections | 99515 | 4296 |
<I/σ(I)> | 19.54 | 2.01 |
Completeness [%] | 99.4 | |
Redundancy | 4.3 | |
CC(1/2) | 0.770 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 10% PEG20000, 100 mM sodium citrate, pH 5.0, and 200 mM MgCl2 |