6VN3
USP7 IN COMPLEX WITH LIGAND COMPOUND 23
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99997 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.510, 65.834, 85.077 |
Unit cell angles | 90.00, 94.62, 90.00 |
Refinement procedure
Resolution | 48.047 - 2.730 |
R-factor | 0.2248 |
Rwork | 0.222 |
R-free | 0.28990 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.475 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.800 | 84.800 |
High resolution limit [Å] | 2.730 | 2.730 |
Rmerge | 0.068 | 0.444 |
Rmeas | 0.084 | 0.052 |
Total number of observations | 52057 | |
Number of reflections | 20126 | 81 |
<I/σ(I)> | 10.27 | 29.9 |
Completeness [%] | 96.4 | 97.2 |
Redundancy | 2.6 | 2.6 |
CC(1/2) | 0.995 | 0.995 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | NULL |