6TJU

X-ray structure of C-terminal domain of human T-cell lymphotropic virus type 1 (HTLV-1)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-05-10
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.9795
Spacegroup name	I 41 3 2
Unit cell lengths	97.408, 97.408, 97.408
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.770 - 1.800
Rwork	0.177
R-free	0.24640
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5llj
RMSD bond length	0.012
RMSD bond angle	1.861
Data reduction software	xia2
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.770	1.840
High resolution limit [Å]	1.800	1.800
Rmerge	0.077	0.711
Rmeas	0.095
Rpim	0.055	0.503
Number of reflections	41483	2513
<I/σ(I)>	7.4	1.8
Completeness [%]	100.0
Redundancy	5.4
CC(1/2)	0.993	0.354

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	293	1.2 M ammonium tartrate dibasic, 150 mM NaCl