6TGS
AtNBR1-PB1 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.873 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 43.128, 79.438, 24.135 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.900 - 1.530 |
R-factor | 0.2221 |
Rwork | 0.220 |
R-free | 0.25490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | EMD-10499 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.900 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_3500: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.900 | 1.585 |
High resolution limit [Å] | 1.530 | 1.530 |
Rmerge | 0.028 | 0.413 |
Rmeas | 0.584 | |
Rpim | 0.028 | 0.413 |
Number of reflections | 12367 | 1271 |
<I/σ(I)> | 10.45 | 1.42 |
Completeness [%] | 99.2 | |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.655 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M MES (pH 6.5), 18-20% (w/v) PEG20000 |