6SNJ

Solution structure of the FUS/TLS RNA recognition motif in complex with U1 snRNA stem loop III

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		600
2	Bruker	AVANCE III		700
3	Bruker	AVANCE		900

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D 1H-13C NOESY aromatic
11	1	2	3D 1H-13C NOESY aliphatic
12	1	1	3D 1H-13C NOESY aromatic
13	1	1	3D 1H-13C NOESY aliphatic
14	1	1	3D 1H-15N NOESY
15	1	4	2D 1H-1H NOESY
16	1	1	3D HNCA
17	1	1	3D HNCO
18	1	1	3D CBCA(CO)NH
19	1	1	3D HNCACB
2	1	1	2D 1H-13C HSQC aliphatic
20	1	2	2D F1fF2F TOCSY
21	1	2	2D F2F NOEY
22	1	2	2D F1FF2f NOESY
23	1	3	3D 1H-13C filtered edited NOESY HSQC
24	1	2	3D 1H-13C filtered edited NOESY HSQC
3	1	1	2D 1H-13C HSQC aromatic
4	1	2	2D 1H-13C HSQC aliphatic
5	1	2	2D 1H-13C HSQC aromatic
6	1	3	3D HCCH-TOCSY
7	1	3	3D 1H-13C NOESY
8	1	3	2D 1H-13C HSQC aromatic
9	1	3	2D 1H-13C HSQC aliphatic

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.8	atm	303

Conformers

Conformers Calculated Total Number	50
Conformers Submitted Total Number	18