6RCO
PfRH5-binding monoclonal antibody R5.004
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9999 |
Spacegroup name | P 1 |
Unit cell lengths | 55.210, 70.180, 73.260 |
Unit cell angles | 101.42, 92.97, 112.47 |
Refinement procedure
Resolution | 42.450 - 1.660 |
R-factor | 0.184 |
Rwork | 0.183 |
R-free | 0.20400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.090 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.450 | 1.690 |
High resolution limit [Å] | 1.660 | 1.660 |
Number of reflections | 111530 | 5493 |
<I/σ(I)> | 8.6 | |
Completeness [%] | 95.7 | |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2 M lithium sulfate, 0.1 M NaAc pH 4.5, 30% PEG 8000 0.33% hexamminecobalt(III) chloride, 0.06 M MES monohydrate, 0.06 PIPES, 0.02 M HEPES chloride |