6QWY
HEWL lysozyme, crystallized from NaCl solution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | KURCHATOV SNC BEAMLINE K4.4 |
Synchrotron site | KURCHATOV SNC |
Beamline | K4.4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-05-28 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.80241 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.147, 77.147, 37.139 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.280 - 1.350 |
R-factor | 0.16044 |
Rwork | 0.158 |
R-free | 0.19850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wld |
RMSD bond length | 0.011 |
RMSD bond angle | 1.599 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.280 | 1.385 |
High resolution limit [Å] | 1.350 | 1.350 |
Rmerge | 0.099 | |
Number of reflections | 25204 | |
<I/σ(I)> | 16.1 | |
Completeness [%] | 100.0 | |
Redundancy | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | NaCl |