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6P0K

Crystal structure of GDP-bound human RalA in a covalent complex with aryl sulfonyl fluoride compounds.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 4.2.2
Synchrotron siteALS
Beamline4.2.2
Temperature [K]100
Detector technologyCMOS
Collection date2019-03-22
DetectorRDI CMOS_8M
Wavelength(s)0.97625
Spacegroup nameC 2 2 21
Unit cell lengths65.281, 104.924, 55.409
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.190 - 1.490
R-factor0.1318
Rwork0.130
R-free0.16410
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1u8z
RMSD bond length0.009
RMSD bond angle1.038
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX (1.15_3459)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]39.1901.540
High resolution limit [Å]1.4901.490
Rmeas0.0881.602
Rpim0.0330.593
Number of reflections315462688
<I/σ(I)>16.31.5
Completeness [%]100.0100
Redundancy7.27.1
CC(1/2)0.7280.728
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.52930.2 M Calcium Acetate pH 5.5 18-22% PEG3350

221051

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