6OVM
Crystal Structure of the Pseudomonas capeferrum Anti-sigma Regulator PupR C-terminal Cell-surface Signaling Domain in Complex with the Outer Membrane Transporter PupB N-terminal Signaling Domain (SeMet)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-08 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.574, 44.714, 141.282 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.630 - 1.600 |
R-factor | 0.1541 |
Rwork | 0.153 |
R-free | 0.18370 |
Structure solution method | SAD |
RMSD bond angle | 1.349 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 141.340 | 1.530 |
High resolution limit [Å] | 1.510 | 1.510 |
Number of reflections | 68598 | 1511 |
<I/σ(I)> | 18.9 | |
Completeness [%] | 98.0 | |
Redundancy | 5.9 | |
CC(1/2) | 0.999 | 0.765 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 200mM sodium potassium tartrate, 20% PEG 3350 |