6MU5
Bst DNA polymerase I TNA/DNA binary complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-06-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 87.390, 93.280, 103.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.839 - 1.912 |
R-factor | 0.1918 |
Rwork | 0.191 |
R-free | 0.22510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l3s |
RMSD bond length | 0.007 |
RMSD bond angle | 0.976 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.840 | 1.980 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.718 | 2.130 |
Number of reflections | 65358 | |
<I/σ(I)> | 41.14 | |
Completeness [%] | 98.7 | |
Redundancy | 19.7 | |
CC(1/2) | 0.821 | 0.821 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 50% ammonium sulfate, 0.1M MES, 2% MPD |