6ML6
ZBTB24 Zinc Fingers 4-8 with 19+1mer DNA Oligonucleotide (Sequence 4 with a CpA 5mC Modification)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-003 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-08-07 |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.163, 68.244, 49.259 |
Unit cell angles | 90.00, 92.90, 90.00 |
Refinement procedure
Resolution | 28.038 - 1.540 |
R-factor | 0.2023 |
Rwork | 0.202 |
R-free | 0.22150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ml5 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.538 |
Data reduction software | CrysalisPro |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.040 | 1.600 |
High resolution limit [Å] | 1.540 | 1.540 |
Rmerge | 0.074 | |
Rpim | 0.036 | 0.724 |
Number of reflections | 45159 | 4490 |
<I/σ(I)> | 9.6 | 0.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 4.7 | |
CC(1/2) | 0.392 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 292 | 25% PEG3350, 0.1 M Bis-Tris, pH 5.5, 0.2 M ammonium acetate |