6MKB
Crystal structure of murine 4-1BB ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97 |
Spacegroup name | P 31 |
Unit cell lengths | 77.362, 77.362, 118.236 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.140 - 2.500 |
R-factor | 0.191 |
Rwork | 0.188 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6d3n |
RMSD bond length | 0.009 |
RMSD bond angle | 1.180 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 5.380 | 2.500 |
Rmerge | 0.077 | 0.050 | 0.791 |
Rmeas | 0.081 | 0.053 | 0.832 |
Rpim | 0.025 | 0.016 | 0.256 |
Number of reflections | 27191 | 2730 | 2727 |
<I/σ(I)> | 4.9 | ||
Completeness [%] | 99.7 | 99.8 | 99.9 |
Redundancy | 10.4 | 10.5 | 10.4 |
CC(1/2) | 0.995 | 0.827 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 2.4 M Ammonium sulfate, 0.1M MES pH 6.0 |