6L30
Crystal structure of the epithelial cell transforming 2 (ECT2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 103 |
Detector technology | CCD |
Collection date | 2015-05-05 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.987 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 106.959, 130.579, 131.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.851 | 2.928 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 23040 | 2692 |
<I/σ(I)> | 21.42 | |
Completeness [%] | 99.8 | |
Redundancy | 6.1 | |
CC(1/2) | 0.720 | 0.717 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 291 | 0.95-1.05 M Potassium/Sodium Tartrate 0.2 M Lithium Sulfate 1 mM TCEP |