6JRB
ZHD/W183F complex with bZOL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97776 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.689, 90.407, 113.148 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.000 - 1.800 |
R-factor | 0.14518 |
Rwork | 0.144 |
R-free | 0.16971 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5c8z |
RMSD bond length | 0.014 |
RMSD bond angle | 1.746 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmeas | 0.101 | 0.693 |
Rpim | 0.027 | 0.198 |
Number of reflections | 71121 | 3514 |
<I/σ(I)> | 29.1 | |
Completeness [%] | 99.3 | |
Redundancy | 13.3 | |
CC(1/2) | 0.973 | 0.898 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | ammonium phosphate, imidazole, potassium chloride |