6J86
Crystal structure of HinD with NMFT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE TPS 05A |
Synchrotron site | NSRRC |
Beamline | TPS 05A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-08-30 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.320, 152.578, 56.336 |
Unit cell angles | 90.00, 115.96, 90.00 |
Refinement procedure
Resolution | 48.073 - 2.600 |
R-factor | 0.1711 |
Rwork | 0.163 |
R-free | 0.24510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6j82 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.039 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.073 | 2.720 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.124 | 0.549 |
Number of reflections | 22845 | 2793 |
<I/σ(I)> | 8.9 | 2.3 |
Completeness [%] | 99.3 | 99.1 |
Redundancy | 3.9 | 3.9 |
CC(1/2) | 0.989 | 0.722 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM MES (pH 6.5) containing 1200 mM (NH4)2HPO4 and 100 mM NaCl |