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6IEP

GAPDH of Streptococcus agalactiae

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsELETTRA BEAMLINE 5.2R
Synchrotron siteELETTRA
Beamline5.2R
Temperature [K]100
Detector technologyPIXEL
Collection date2014-11-18
DetectorDECTRIS PILATUS 2M
Wavelength(s)0.9790
Spacegroup nameP 21 21 21
Unit cell lengths88.580, 124.420, 125.310
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 2.600
R-factor0.206
Rwork0.206
R-free0.24600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3k73
RMSD bond length0.007
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareREFMAC
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]36.1702.740
High resolution limit [Å]2.6002.600
Rmerge0.1570.430
Rmeas0.1700.475
Rpim0.0490.152
Number of reflections43229
<I/σ(I)>135.7
Completeness [%]99.9
Redundancy11.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP28740% PEG 4000 monomethyl ether and 100 mM Tris-HCl pH 9.0

221051

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