6I0S
Crystal structure of DmTailor in complex with UMPNPP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-03 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.00767 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 61.183, 61.183, 167.380 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.768 - 1.900 |
R-factor | 0.1897 |
Rwork | 0.188 |
R-free | 0.21880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5w0b |
RMSD bond length | 0.011 |
RMSD bond angle | 0.884 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.770 | 2.010 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 29527 | |
<I/σ(I)> | 15.81 | 1.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 19.6 | 19 |
CC(1/2) | 0.999 | 0.534 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 20 % (v/v) glycerol ethoxylate |