6HXT
Crystal structure of the head domain of human CCDC61
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-12-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 36.877, 68.222, 180.728 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.680 - 2.550 |
R-factor | 0.2131 |
Rwork | 0.208 |
R-free | 0.25600 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 1.080 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.680 | 2.660 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.077 | 0.568 |
Rmeas | 0.086 | 0.630 |
Rpim | 0.037 | 0.266 |
Number of reflections | 15498 | 1872 |
<I/σ(I)> | 14.7 | |
Completeness [%] | 99.1 | 99.7 |
Redundancy | 5 | 5.2 |
CC(1/2) | 0.998 | 0.932 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 293 | 8%(w/v) PEG6,000, 100 mM Tris-HC |