6HNS
Structure of Nitrincola lacisaponensis flavin-containing monooxygenase (FMO) in complex with FAD and NADP+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-23 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.000040 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 59.057, 125.611, 144.725 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.480 - 1.840 |
R-factor | 0.18325 |
Rwork | 0.181 |
R-free | 0.21724 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vq7 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.616 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.480 | 1.870 |
High resolution limit [Å] | 1.840 | 1.840 |
Rmerge | 0.076 | 0.849 |
Number of reflections | 93414 | 4431 |
<I/σ(I)> | 14.7 | |
Completeness [%] | 99.2 | 97.1 |
Redundancy | 4.4 | 4.4 |
CC(1/2) | 0.999 | 0.585 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 8 | 277 | 0.2 Mg formate, 20% W/V PEG3350 |