6HJL
Affimer:BclxL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9174 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 68.270, 87.290, 112.180 |
Unit cell angles | 90.00, 96.18, 90.00 |
Refinement procedure
Resolution | 55.760 - 2.200 |
R-factor | 0.21753 |
Rwork | 0.215 |
R-free | 0.26664 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.548 |
Data reduction software | xia2 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.760 | 2.300 |
High resolution limit [Å] | 2.200 | 2.240 |
Number of reflections | 62008 | |
<I/σ(I)> | 4.1 | |
Completeness [%] | 98.1 | |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | MPD |