6HAP
Adenylate kinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2017-09-25 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5417 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 73.560, 76.840, 86.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.490 - 2.700 |
R-factor | 0.2263 |
Rwork | 0.224 |
R-free | 0.27760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4jzk |
RMSD bond length | 0.006 |
RMSD bond angle | 2.291 |
Data reduction software | iMOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1-2575_1692: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.490 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 7058 | 696 |
<I/σ(I)> | 16.48 | |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 5.8 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 10% PEG 3350 0.05M Tris pH=5.5 |