6H5V
MamM CTD H264E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-20 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97624 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 37.179, 94.367, 53.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.180 - 1.490 |
R-factor | 0.20116 |
Rwork | 0.200 |
R-free | 0.22878 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3w5x |
RMSD bond length | 0.010 |
RMSD bond angle | 1.437 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0171) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.180 | 1.520 |
High resolution limit [Å] | 1.490 | 1.490 |
Rmerge | 0.065 | |
Number of reflections | 15616 | |
<I/σ(I)> | 13.9 | |
Completeness [%] | 99.6 | |
Redundancy | 8.6 | |
CC(1/2) | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M Ammonium sulfate, 0.1M BIS-TRIS pH=5.5, 25% PEG 3350, 1.7 mM MnCl2 |