6G0V
Human Galectin-3 in complex with a TF tumor-associated antigen mimetic
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-12 |
Detector | DECTRIS PILATUS3 R CdTe 300K |
Wavelength(s) | 0.9677 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 35.900, 58.200, 62.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.675 - 1.090 |
R-factor | 0.1541 |
Rwork | 0.153 |
R-free | 0.17710 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.035 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.675 | 1.140 |
High resolution limit [Å] | 1.090 | 1.090 |
Rmerge | 0.040 | |
Rpim | 0.019 | |
Number of reflections | 41602 | |
<I/σ(I)> | 17.8 | |
Completeness [%] | 76.2 | |
Redundancy | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 34% (w/v) PEG 400, 100 mM Tris-HCl (pH 7.5), 100 mM MgCl2, 8 mM B-mercaptoethanol |