6FK6
Crystal structure of N2C/D282C stabilized opsin bound to RS01
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-21 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.000020 |
Spacegroup name | H 3 2 |
Unit cell lengths | 244.209, 244.209, 111.752 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.790 - 2.360 |
R-factor | 0.216 |
Rwork | 0.216 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | INHOUSE MODEL |
RMSD bond length | 0.004 |
RMSD bond angle | 0.772 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.10_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.790 | 2.420 |
High resolution limit [Å] | 2.360 | 2.360 |
Rmerge | 0.114 | 5.370 |
Number of reflections | 52217 | |
<I/σ(I)> | 15.39 | 0.55 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.43 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | AMMONIUM SULPHATE, SODIUM ACETATE, D(+)-TREHALOSE, PH 6.0 |