6ERN
HIV Hexamer with ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 277 |
| Detector technology | CCD |
| Collection date | 2017-01-03 |
| Detector | OXFORD RUBY CCD |
| Wavelength(s) | 1 |
| Spacegroup name | P 6 |
| Unit cell lengths | 90.846, 90.846, 56.747 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 78.670 - 2.360 |
| R-factor | 0.18709 |
| Rwork | 0.185 |
| R-free | 0.23665 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.825 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASES |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 78.680 |
| High resolution limit [Å] | 2.359 |
| Number of reflections | 11142 |
| <I/σ(I)> | 15.4 |
| Completeness [%] | 91.0 |
| Redundancy | 4.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 277 | PEG4K |
