6EOA
Crystal Structure of HAL3 from Cryptococcus neoformans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-15 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9792 |
Spacegroup name | H 3 2 |
Unit cell lengths | 88.194, 88.194, 165.774 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.168 - 2.180 |
R-factor | 0.2158 |
Rwork | 0.214 |
R-free | 0.23910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e20 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.883 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.170 | 2.290 |
High resolution limit [Å] | 2.180 | 2.180 |
Rmerge | 0.062 | |
Rmeas | 0.068 | |
Rpim | 0.030 | |
Number of reflections | 12855 | 1694 |
<I/σ(I)> | 17.2 | |
Completeness [%] | 96.5 | 89.2 |
Redundancy | 9.4 | 6.9 |
CC(1/2) | 0.990 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 291 | 0.8M Succinic acid, pH 7.0 |