6DSR

Re-refinement of P. falciparum orotidine 5'-monophosphate decarboxylase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL38B1
Synchrotron site	SPring-8
Beamline	BL38B1
Temperature [K]	93
Detector technology	CCD
Collection date	2006-11-18
Detector	ADSC QUANTUM 315
Wavelength(s)	1
Spacegroup name	H 3
Unit cell lengths	201.879, 201.879, 44.191
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	36.734 - 2.597
R-factor	0.1846
Rwork	0.182
R-free	0.22440
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3n3m
RMSD bond length	0.004
RMSD bond angle	0.715
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.10.1_2155)

Data quality characteristics

	Overall
Low resolution limit [Å]	36.734
High resolution limit [Å]	2.597
Number of reflections	20677
<I/σ(I)>	4
Completeness [%]	98.8
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9.5	293	23% PEG 3000, pH 9.5