6DK9
Yeast Ddi2 Cyanamide Hydratase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08B1-1 |
Synchrotron site | CLSI |
Beamline | 08B1-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-08-15 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 1.12713 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 264.456, 264.456, 119.152 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.700 - 2.600 |
R-factor | 0.2014 |
Rwork | 0.201 |
R-free | 0.21680 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 0.812 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.700 | 2.640 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.105 | 0.695 |
Number of reflections | 144816 | 7127 |
<I/σ(I)> | 17.6 | 2.9 |
Completeness [%] | 99.0 | 97.9 |
Redundancy | 7.7 | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 1.1-1.3 M Ammonium Sulfate 0.2 M Arginine 0.1 M N-morpholino ethane sulfonate pH 5.6 |