6D8N
Group I self-splicing intron P4-P6 domain mutant G134A/U185AA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-22 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.979300 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.650, 130.880, 146.430 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.142 - 3.954 |
R-factor | 0.247275138779 |
Rwork | 0.246 |
R-free | 0.26551 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1gid |
RMSD bond length | 0.003 |
RMSD bond angle | 0.500 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 66.200 |
High resolution limit [Å] | 3.950 |
Number of reflections | 13327 |
<I/σ(I)> | 15.6 |
Completeness [%] | 99.5 |
Redundancy | 12.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | MPD, sodium cacodylate, spermine |