6BZP
STGGYG from low-complexity domain of FUS, residues 77-82
Experimental procedure
Source type | ELECTRON MICROSCOPE |
Source details | TECNAI F20 TEM |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2015-08-18 |
Detector | TVIPS F416 CMOS CAMERA |
Wavelength(s) | 0.0251 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 13.790, 4.930, 101.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 13.310 - 1.100 |
R-factor | 0.223 |
Rwork | 0.219 |
R-free | 0.25500 |
Structure solution method | AB INITIO PHASING |
RMSD bond length | 0.013 |
RMSD bond angle | 1.060 |
Data scaling software | XSCALE |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 13.310 | 13.310 | 1.130 |
High resolution limit [Å] | 1.100 | 4.920 | 1.100 |
Rmerge | 0.250 | 0.135 | 0.553 |
Rmeas | 0.266 | 0.162 | 0.629 |
Total number of observations | 23271 | ||
Number of reflections | 3220 | 41 | 197 |
<I/σ(I)> | 4.15 | 4.75 | 1.46 |
Completeness [%] | 95.5 | 91.1 | 74.9 |
Redundancy | 7.227 | 2.854 | 3.939 |
CC(1/2) | 0.985 | 0.988 | 0.729 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 298 | 0.1 M sodium acetate, pH 4.6, 0.15 M ammonium sulfate, 25% w/v PEG2000 MME |