6ARC
Monoclinic EutL - structure determined from merged "Group 1" data
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-10-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9791 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 118.740, 66.140, 80.140 |
Unit cell angles | 90.00, 108.53, 90.00 |
Refinement procedure
Resolution | 19.804 - 1.900 |
R-factor | 0.1387 |
Rwork | 0.137 |
R-free | 0.18140 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 0.990 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2686: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.804 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 43719 | |
<I/σ(I)> | 20.96 | 4.35 |
Completeness [%] | 94.0 | 96 |
Redundancy | 17.4 | 4.8 |
CC(1/2) | 0.998 | 0.897 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 298 | 0.1M sodium potassium phosphate, 0.25 sodium chloride, 10% PEG 8000 |