5XP7
C-Src in complex with ATP-CHCl
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2016-12-21 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 |
Unit cell lengths | 42.276, 63.978, 74.003 |
Unit cell angles | 101.03, 89.83, 90.60 |
Refinement procedure
Resolution | 36.551 - 2.012 |
R-factor | 0.1692 |
Rwork | 0.168 |
R-free | 0.19820 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.205 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 36.600 |
High resolution limit [Å] | 2.000 |
Number of reflections | 48688 |
<I/σ(I)> | 13.9 |
Completeness [%] | 96.5 |
Redundancy | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG4000 |