5XP5
C-Src in complex with ATP-Chf
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2014-01-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 |
Unit cell lengths | 42.288, 63.687, 73.815 |
Unit cell angles | 79.07, 89.23, 89.24 |
Refinement procedure
Resolution | 43.446 - 2.101 |
R-factor | 0.2191 |
Rwork | 0.218 |
R-free | 0.24620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4u5j |
RMSD bond length | 0.004 |
RMSD bond angle | 0.854 |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.500 | 2.110 |
High resolution limit [Å] | 2.100 | 2.070 |
Rpim | 0.057 | |
Number of reflections | 41453 | 299 |
<I/σ(I)> | 15.18 | |
Completeness [%] | 94.1 | |
Redundancy | 10 | 1.8 |
CC(1/2) | 0.313 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG 4000 |