Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-04-23 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.654, 45.214, 70.721 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.854 - 1.951 |
R-factor | 0.1984 |
Rwork | 0.196 |
R-free | 0.24140 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.145 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.950 |
Number of reflections | 9978 |
<I/σ(I)> | 19.2 |
Completeness [%] | 93.2 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 4M ammonium acetate, 0.1M sodium acetate |