5X4T

PAC from Oscillatoria acuminata after 20 seconds photoactivation

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	100
Detector technology	CCD
Collection date	2016-05-16
Detector	ADSC QUANTUM 270
Wavelength(s)	1.00
Spacegroup name	P 61 2 2
Unit cell lengths	77.083, 77.083, 205.376
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	31.743 - 1.601
R-factor	0.212
Rwork	0.210
R-free	0.24640
RMSD bond length	0.007
RMSD bond angle	0.907
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	PHENIX ((1.10.1_2155))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.600
Number of reflections	46919
<I/σ(I)>	17
Completeness [%]	96.7
Redundancy	10.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5	293	100mM Sodium Citrate pH 5.0, 10% PEG 20000, 5mM ApCpp, 2mM MgCl2