5W5H
Human IFIT1 dimer with m7Gppp-AAAA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 94 |
Detector technology | CCD |
Collection date | 2016-01-16 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.979 |
Spacegroup name | I 4 |
Unit cell lengths | 184.355, 184.355, 88.762 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.010 - 2.790 |
R-factor | 0.22 |
Rwork | 0.219 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.702 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2142: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.840 |
High resolution limit [Å] | 2.790 | 2.790 |
Rpim | 0.028 | 0.512 |
Number of reflections | 37109 | |
<I/σ(I)> | 26.1 | 1.72 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 5.1 | 5 |
CC(1/2) | 0.790 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.1 | 277.15 | 27 - 32 % PEG 200, 0.1 M Tris pH 8.1, 200 mM CaCl2 |