5VTH
CTX-M-14 P167S:E166A mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-04-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9999 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 41.690, 41.690, 233.052 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.690 - 2.200 |
R-factor | 0.2221 |
Rwork | 0.220 |
R-free | 0.26840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ylt |
RMSD bond length | 0.004 |
RMSD bond angle | 0.605 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless (0.5.31) |
Phasing software | PHASER (2.7.17) |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.690 | |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.130 | 0.311 |
Rpim | 0.069 | 0.150 |
Number of reflections | 21502 | |
<I/σ(I)> | 6.56 | |
Completeness [%] | 95.3 | |
Redundancy | 2 | |
CC(1/2) | 0.993 | 0.954 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1M MES pH6.5, 25% (w/v) PEG 4000 |