5UDE
Crystal Structure of RSV F B9320 DS-Cav1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97918 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 170.430, 170.430, 170.430 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.608 - 3.001 |
R-factor | 0.1946 |
Rwork | 0.193 |
R-free | 0.23380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4mms |
RMSD bond length | 0.006 |
RMSD bond angle | 0.781 |
Data reduction software | MOSFLM |
Data scaling software | Aimless (0.3.6) |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.610 | 42.610 | 3.210 |
High resolution limit [Å] | 3.000 | 8.490 | 3.000 |
Rmerge | 0.209 | 0.050 | 0.972 |
Rmeas | 0.229 | ||
Rpim | 0.093 | ||
Total number of observations | 99952 | ||
Number of reflections | 17606 | ||
<I/σ(I)> | 7.8 | ||
Completeness [%] | 99.5 | 95.7 | 100 |
Redundancy | 5.7 | 5.1 | 5.6 |
CC(1/2) | 0.988 | 0.997 | 0.659 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 20% w/v PEG1500, 0.1 M Tris pH 7.5, 0.1 M ammonium sulfate |