5U9Z
Phosphoglycerol transferase GacH from Streptococcus pyogenes
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-12-15 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 0.97933 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.870, 78.170, 172.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.506 - 2.001 |
R-factor | 0.2162 |
Rwork | 0.215 |
R-free | 0.23950 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.549 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.7.12) |
Refinement software | PHENIX (dev_2481) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.506 | 49.506 | 2.050 |
High resolution limit [Å] | 2.000 | 8.950 | 2.000 |
Rmerge | 0.083 | 0.077 | 0.827 |
Rmeas | 0.097 | ||
Total number of observations | 430511 | ||
Number of reflections | 119913 | ||
<I/σ(I)> | 8.5 | 18.42 | 1.11 |
Completeness [%] | 98.7 | 99.5 | 90 |
Redundancy | 3.59 | 3.664 | 2.469 |
CC(1/2) | 0.993 | 0.986 | 0.614 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 294 | 0.1M HEPES pH 7.5, 10% PEG8000, 8% ethylene glycol |