5N6F
Crystal structure of TGT in complex with guanine fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-01-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.918 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 88.711, 64.851, 70.655 |
Unit cell angles | 90.00, 93.36, 90.00 |
Refinement procedure
Resolution | 44.279 - 1.119 |
R-factor | 0.136782737006 |
Rwork | 0.136 |
R-free | 0.15350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4lbu |
RMSD bond length | 0.007 |
RMSD bond angle | 0.962 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.280 | 1.190 |
High resolution limit [Å] | 1.119 | 1.119 |
Rmerge | 0.487 | |
Number of reflections | 149008 | 149008 |
<I/σ(I)> | 10.3 | 1.96 |
Completeness [%] | 97.1 | 83.2 |
Redundancy | 3.6 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 289 | 13% PEG8000, 100MM MES, 1MM DTT, 10% DMSO |