5LX9
CRYSTAL STRUCTURE OF HUMAN ADIPONECTIN RECEPTOR 2 IN COMPLEX WITH A C18 FREE FATTY ACID AT 2.4 ANGSTROM RESOLUTION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-30 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.976251 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 74.578, 101.128, 111.577 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 101.130 - 2.400 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.20500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.050 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 101.130 | 2.500 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.527 | 5.681 |
Number of reflections | 33584 | |
<I/σ(I)> | 5.5 | 1.1 |
Completeness [%] | 100.0 | 99.7 |
Redundancy | 10.5 | 10.2 |
CC(1/2) | 0.988 | 0.489 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 293 | 30-45% PEG 400, 0.1 M HEPES pH 7.0, and 50-100 mM potassium citrate, 0.01 mM AdipoRon |