5LW4

NMR solution structure of the apo-form of the chitin-active lytic polysaccharide monooxygenase BlLPMO10A

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		600
2	Bruker	Ascend		800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	3	3D HCCH-TOCSY
11	1	3	2D (HB)CB(CGCD)HD
12	1	3	2D CACO
13	1	3	2D CON
14	1	1	3D 1H-15N NOESY
15	1	2	3D 1H-15N NOESY
16	1	2	3D 1H-13C NOESY aliphatic
17	1	2	3D 1H-13C NOESY aromatic
18	1	2	3D 1H-13C NOESY aliphatic
2	1	2	2D 1H-13C HSQC aliphatic
3	1	2	2D 1H-13C HSQC aromatic
4	1	2	3D HNCO
5	1	2	3D HN(CA)CO
6	1	2	3D HNCA
7	1	2	3D HBHA(CO)NH
8	1	2	3D CBCA(CO)NH
9	1	2	3D CBCANH

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5	1	298

Conformers

Conformers Calculated Total Number	259
Conformers Submitted Total Number	20