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5L6Q

Refolded AL protein from cardiac amyloidosis

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2014-12-01
DetectorPSI PILATUS 6M
Wavelength(s)1.0
Spacegroup nameP 21 21 2
Unit cell lengths58.020, 105.810, 34.750
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 1.400
R-factor0.14904
Rwork0.147
R-free0.18208
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4od2
RMSD bond length0.014
RMSD bond angle1.668
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0135)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.500
High resolution limit [Å]1.4001.400
Rmerge0.0540.525
Number of reflections42100
<I/σ(I)>12.62.6
Completeness [%]97.698.7
Redundancy4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52930.1 M MES, 18% PEG 8000, 0.1 M Zinc acetate

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