5HOO
Crystal structure of the Mos1 Strand Transfer Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 256.340, 58.830, 110.140 |
Unit cell angles | 90.00, 94.91, 90.00 |
Refinement procedure
Resolution | 60.010 - 3.300 |
R-factor | 0.2339 |
Rwork | 0.232 |
R-free | 0.27390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3hos |
RMSD bond length | 0.008 |
RMSD bond angle | 1.255 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.990 | 3.520 |
High resolution limit [Å] | 3.290 | 3.290 |
Number of reflections | 25201 | |
<I/σ(I)> | 8.1 | 3.3 |
Completeness [%] | 99.6 | 99.5 |
Redundancy | 3.1 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 290 | 30% (v/v) MPD, 0.1 M sodium cacodylate pH 6.5,0.2 M magnesium acetate tetrahydrate |