5HO3
MamB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-06-13 |
Detector | MARRESEARCH |
Wavelength(s) | 0.932 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 97.364, 37.600, 49.652 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.650 - 2.150 |
R-factor | 0.2046 |
Rwork | 0.200 |
R-free | 0.24548 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3w5x |
RMSD bond length | 0.014 |
RMSD bond angle | 1.647 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.650 | |
High resolution limit [Å] | 2.150 | |
Rmerge | 0.048 | 0.449 |
Number of reflections | 10470 | |
<I/σ(I)> | 38.03 | |
Completeness [%] | 99.2 | |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 293.15 | 0.1 M HEPES pH 7.5, 25% PEG 3350, 0.2 M LiSO4 |