5H49

Crystal structure of Cbln1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2014-10-31
Detector	RAYONIX MX-325
Wavelength(s)	0.9795
Spacegroup name	P 43 21 2
Unit cell lengths	91.638, 91.638, 151.046
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.800
R-factor	0.27318
Rwork	0.271
R-free	0.30696
RMSD bond length	0.004
RMSD bond angle	1.004
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	REFMAC (5.8.0155)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.800
Number of reflections	16418
<I/σ(I)>	15.3
Completeness [%]	99.8
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	0.1 M Na/K phosphate, pH 6.2, 2.5 M NaCl