5GOX
Eukaryotic Rad50 Functions as A Rod-shaped Dimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9766 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.180, 61.972, 81.540 |
Unit cell angles | 90.00, 99.75, 90.00 |
Refinement procedure
Resolution | 28.221 - 2.405 |
R-factor | 0.2164 |
Rwork | 0.213 |
R-free | 0.27090 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.302 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (dev_1745) |
Refinement software | PHENIX (dev_1745) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.440 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 16270 | |
<I/σ(I)> | 42.2 | |
Completeness [%] | 99.6 | |
Redundancy | 6.9 | |
CC(1/2) | 0.980 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.7 | 291 | 28 - 30% PEG 600, 0.1 M bis-tris propane, 3% 1, 6-hexanediol, 5 mM DTT |