5F0U
Crystal structure of Gold binding protein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-07-18 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5419 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 37.095, 37.095, 170.032 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.130 - 1.680 |
R-factor | 0.19884 |
Rwork | 0.197 |
R-free | 0.22699 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.582 |
Data reduction software | HKL-3000 |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.710 |
High resolution limit [Å] | 1.680 | 1.680 |
Number of reflections | 8466 | |
<I/σ(I)> | 24.31 | 3.756 |
Completeness [%] | 98.0 | |
Redundancy | 11.6 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 2.0 M Ammonium citrate tribasic, 0.1 M BIS-TRIS propane |