5CCO
Staphylococcus bacteriophage 80alpha dUTPase with dUMP.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-26 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 3 |
Unit cell lengths | 87.000, 87.000, 87.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 61.520 - 2.330 |
R-factor | 0.20322 |
Rwork | 0.201 |
R-free | 0.24437 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zez |
RMSD bond length | 0.012 |
RMSD bond angle | 1.633 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0107) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.520 | 2.460 |
High resolution limit [Å] | 2.330 | 2.330 |
Rmerge | 0.100 | |
Number of reflections | 9645 | |
<I/σ(I)> | 16.2 | 6.2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 11 | 10.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 294 | 60% ethanol, 0.1 M NaCl |